| 摘要 |
The method according to the invention is based on obtaining selective packing for liquid chromatography in a reversed system of phases containing alkyl-phosphate ligands according to formula 1, where R denotes an alkyl chain. For this purpose, a multi-stage reaction among an amine phase, phosphorus(V) trichloride oxide, and an alcohol in favourable conditions is performed. The product obtained is separated from the reaction mixture, rinsed and dried. The stationary phases obtained can be successfully applied for separating organic compounds in reverse phases systems in liquid chromatography and for extracting to a stationary phase. |
