发明名称 |
METHOD FOR PRODUCING (METH)ACRYLATE ESTER |
摘要 |
<p>Disclosed is a method for producing a (meth)acrylate ester wherein a high purity (meth)acrylate ester is obtained with a high yield, with a reduced loss of (meth)acrylic acid anhydride. In the method, (meth)acrylic acid is recovered with a high yield, and the (meth)acrylate ester is purified easily. Specifically disclosed is a method for producing a (meth)acrylate ester which comprises: (1) a step of producing (meth)acrylic acid anhydride by reacting a specific fatty acid anhydride and (meth)acrylic acid, while removing a by-produced fatty acid; (2) a step of obtaining a (meth)acrylate ester by reacting an alcohol and unpurified (meth)acrylic acid anhydride obtained in step (1) preferably at a temperature not less than 90 °C; and (3) a step of recovering (meth)acrylic acid by distillation preferably at a temperature not less than 90 °C. The method may also comprise a step of heating or distilling the reaction liquid obtained in step (2) at a temperature not less than 90 °C.</p> |
申请公布号 |
EP2399898(A1) |
申请公布日期 |
2011.12.28 |
申请号 |
EP20100738589 |
申请日期 |
2010.02.04 |
申请人 |
MITSUBISHI RAYON CO., LTD. |
发明人 |
ANSAI, RYUICHI;NOGAMI, HIROYUKI;OGURA, KUNIYOSHI |
分类号 |
C07C67/08;C07C67/54;C07C69/54 |
主分类号 |
C07C67/08 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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