METHOD OF PRODUCING ACYL FLUORIDE OF PERFLUOROCYCLOHEXANE CARBOXYLIC ACID

摘要

FIELD: chemistry. ^ SUBSTANCE: method of producing acyl fluoride perfluorocyclohexane carboxylic acid is realised via electrochemical fluorination of acyl chloride of benzoic acid in liquid anhydrous hydrogen fluoride on nickel anodes in the presence of an electrolyte additive, where the said additive is triallyl amine and the electrolysis process is carried out with pulsed electric current, where electrolysis is carried out in an electrolysis cell with a self-contained separator of the crude material collector. ^ EFFECT: longer service life of the electrolyte. ^ 2 cl, 1 tbl, 5 ex