摘要 |
The invention relates to a method for producing 6-chlorodibenzo[d,f] [1,3,2]-dioxaphosphepin (formula 1), comprising the following steps: a) addition of liquid 2,2′-dihydroxybiphenyl into a reactor to an excess of phosphorous trichloride under inert gas and stirring; b) discharge and neutralization of the resulting gases from the reaction mixture; c) separation of the excess phosphorous trichloride; d) obtention of 6-chlorodibenzo[d,f] [1,3,2]-dioxaphosphepin.
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