发明名称 Process for producing triphenylene compound and crystal obtained by the process
摘要 An object of the present invention is to provide a process for producing high-purity hydroxytriphenylenes in which not only inexpensive raw materials can be used but also no complicated steps of deprotection such as dealkylation, and reduction and the like are necessary, and which is thereby advantageous in industrial production. Also there is provided a novel crystal of 2,3,6,7,10,11-hexahydroxytriphenylene monohydrate, which has satisfactory thermal stability. The process for producing a compound represented by the general formula (2) is characterized by reacting a compound represented by the general formula (1) in the presence of a metal oxide comprising a metal selected from trivalent iron, pentavalent vanadium and hexavalent molybdenum and of a nonvolatile strong acid: wherein, Rs are each independently a hydrogen atom, a halogen atom, an alkyl group having 1 to 3 carbon atoms or an alkoxy group having 1 to 3 carbon atoms.
申请公布号 US7964757(B2) 申请公布日期 2011.06.21
申请号 US20080670707 申请日期 2008.08.06
申请人 WAKO PURE CHEMICAL INDUSTRIES, LTD. 发明人 TAKANO DAISUKE;KATO TOMOKAZU;FUJINAKA TOSHIHIRO;SAKAMOTO KAZUNORI
分类号 C07C39/19;C07C37/00 主分类号 C07C39/19
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