| 摘要 |
A method for growing crystals in solution is suitable for the rapid, controlled and effective preparation of crystals of large dimensions from a solution supersaturated with a compound. The crystal growth is carried out under static conditions. To do this: the growth is performed in a crystallisation chamber kept at a constant temperature Tc, which chamber is in fluid communication with a saturation chamber at a temperature Ts, similarly constant and different from Tc, with solubility of the compound at the temperature Ts greater than the solubility of the compound at the temperature Tc. A continuous circulation of the solution between the crystallisation and saturation chambers is established, thus maintaining a constant supersaturation rate within the crystallisation chamber. Furthermore, the circulating solution is subjected to a treatment for eliminating and inhibiting the formation of aggregates, enabling the nucleation of parasitic crystallites to be inhibited. |
