发明名称 METHOD FOR PRODUCING ALKYLENE GLYCOL DI(METH)ACRYLATE
摘要 <P>PROBLEM TO BE SOLVED: To enable an organotin compound catalyst to be recovered and to be repeatedly used in an ester-interchange reaction in good repeatability in a method for producing an alkylene glycol di(meth)acrylate by subjecting an alkyl (meth)acrylate and a hydroxyalkyl (meth)acrylate to the ester-interchange reaction in the presence of the organotin compound catalyst. <P>SOLUTION: The method for producing the alkylene glycol di(meth)acrylate includes reusing the following distillation residue containing the catalytic component in a new ester-interchange reaction by adding and dissolving the hydroxyalkyl (meth)acrylate in the distillation residue, and recycling the mixture. The distillation residue is obtained by distilling a reaction mixture after the ester-interchange reaction to separate the alkylene di(meth)acrylate or the like of a target product, and cooling the distillation residue containing the catalytic component to &le;100&deg;C. <P>COPYRIGHT: (C)2011,JPO&INPIT
申请公布号 JP2011063531(A) 申请公布日期 2011.03.31
申请号 JP20090214357 申请日期 2009.09.16
申请人 NIPPON SHOKUBAI CO LTD 发明人 ISHIDA NORIMASA;TAKAGI HIROYUKI
分类号 C07C67/03;B01J31/22;C07B61/00;C07C69/54 主分类号 C07C67/03
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