发明名称 Rapid synthesis and size control of chalcopyrite-based semi-conductor nanoparticles using microwave irradiation
摘要 CuInS2 nanoparticles have been prepared from single source precursors via microwave irradiation. Also, CuInGaS2 alloy nanoparticles have been prepared. Microwave irradiation methods have allowed an increase in the efficiency of preparation of these materials by providing increased uniformity of heating and shorter reaction times. Nanoparticle growth has been controlled in the about 1 to 5 nm size range by variation of thiolated capping ligand concentrations as well as reaction temperatures and times. Investigation of the photophysical properties of the colloidal nanoparticles has been performed using electronic absorption and luminescence emission spectroscopy. Qualitative nanoparticles sizes have been determined from the photoluminescence (PL) data and compared to TEM images.
申请公布号 US7892519(B2) 申请公布日期 2011.02.22
申请号 US20070957108 申请日期 2007.12.14
申请人 IDAHO STATE UNIVERSITY 发明人 PAK JOSHUA J.;GARDNER JOSEPH S.;SHURDHA ENDRIT;RODRIGUEZ RENE G.;LAU LISA D
分类号 C01B17/00 主分类号 C01B17/00
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