发明名称 |
Biphenyltetracarboxylic acid dianhydride and process for producing the same, and polyimide formed from the same and process for producing the same |
摘要 |
To provide a process for producing BPDA whereby high productivity is attained while high purity is maintained. A process for producing biphenyltetracarboxylic acid dianhydride, which comprises heating biphenyltetracarboxylic acid to produce biphenyltetracarboxylic acid dianhydride, characterized in that the heating is carried out at a pressure of from 1×102 Pa to 1.1×105 Pa to a maximum temperature in a range of from 210° C. to 250° C. in such a manner that the temperature rising rate is higher than 50° C./hr for a period of at least ¼ of the time for the temperature rise from 60° C. to 210° C., and the temperature is maintained to be from 150° C. to 250° C. for from 0.5 to 10 hours.
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申请公布号 |
US7842824(B2) |
申请公布日期 |
2010.11.30 |
申请号 |
US20050570812 |
申请日期 |
2005.06.28 |
申请人 |
MITSUBISHI CHEMICAL CORPORATION |
发明人 |
MIKAMI HIROSHI;NITTA MAKOTO;NOGUCHI NAOKI |
分类号 |
C07D307/89;C08G69/32 |
主分类号 |
C07D307/89 |
代理机构 |
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代理人 |
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地址 |
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