发明名称 2-ETHYLHEXANOL SYNTHESIS METHOD
摘要 FIELD: chemistry. ^ SUBSTANCE: invention relates to a method for synthesis of 2-ethylhexanol by hydrogenating 2-ethylhexenal in liquid phase on an industrial aluminium-nickel-titanium catalyst at temperature of 160-200C, pressure of up to 30 MPa and bulk speed of feeding material of 0.3-0.5 h-1. The process is carried out in two reactors, in each of which 2-ethylhexanal is independently fed with the same bulk speed and a hydrogenation product comes out of each, and after separation from the hydrogenation product after the first reactor circulation hydrogen is fed into the second reactor while simultaneously replenishing it with fresh hydrogen in an amount which ensures the same pressure as hydrogen pressure at the input of the first reactor. ^ EFFECT: method lowers hydrogen consumption owing to reduction of its volume fed for circulation, and improves cost-performance ratio of the process. ^ 2 ex
申请公布号 RU2404955(C1) 申请公布日期 2010.11.27
申请号 RU20090120155 申请日期 2009.05.27
申请人 OBSHCHESTVO S OGRANICHENNOJ OTVETSTVENNOST'JU "OKSOKHIMNEFT'" 发明人 SOKOLOV BORIS GENNAD'EVICH;GIL'CHENOK NAUM DAVYDOVICH;BORISOV RIM BORISOVICH;PETROV ANATOLIJ NIKOLAEVICH;SOKOLOV MAKSIM BORISOVICH
分类号 C07C29/141;C07C31/125 主分类号 C07C29/141
代理机构 代理人
主权项
地址