发明名称 ALUMINUM NITRIDE POWDER, MANUFACTURING METHOD THEREOF, ALUMINUM NITRIDE SINTERED BODY USING THE POWDER, AND MANUFACTURING METHOD OF THE ALUMINUM NITRIDE SINTERED BODY
摘要 PURPOSE: An aluminum nitride powder, a manufacturing method thereof, an aluminum nitride sintered body using the powder, and a manufacturing method of the aluminum nitride sintered body are provided to reduce the amount of residual oxygen by fixing or trapping impurity oxygen. CONSTITUTION: A method for manufacturing aluminum nitride powders comprises the steps of: vaporizing the chloroaluminum stored at an aluminum source storage unit by heating a heating unit; increasing the temperature of a reaction chamber to the temperature which is lower than the nitride thermal treatment temperature by inputting the ammonia gas to 5~100ml flow rate and the nitrogen gas of 50~400ml flow rate into the reaction chamber; increasing the temperature of the reaction chamber to the nitrogen thermal treatment temperature by inputting the ammonia gas to 100~600ml flow rate and the nitrogen gas of 400~800ml flow rate into the reaction chamber; supplying the vaporized chloroaluminum gas into the reaction chamber by supplying nitrogen gas to the aluminum source storage unit; and forming the aluminum nitride powers by chemically reacting the chloroaluminum gas with the ammonia gas.
申请公布号 KR20100112712(A) 申请公布日期 2010.10.20
申请号 KR20090031138 申请日期 2009.04.10
申请人 KOREA INSTITUTE OF CERAMIC ENGINEERING AND TECHNOLOGY 发明人 PEE, JAE HWAN;KIM, SOO RYONG;PARK, JONG CHUL;KIM, YOO JIN
分类号 C01B21/072;C04B35/581 主分类号 C01B21/072
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