| 摘要 |
PROBLEM TO BE SOLVED: To provide a method and an apparatus for preparing metal or non-metal phthalocyanine. SOLUTION: Phthalic anhydride, phthalimide, 1,3-diiminoisoindoline, 1,2-dicyanobenzene, a halogen derivative, an alkyl derivative, or an alkoxy derivative thereof are mixed homogeneously with a metal chloride or an alkoxy metal at 130-250°C for 0.25-15 hr, in the presence of a solvent using microwaves having a frequency of 0.1-1,000 Hz and a power level of 100-3,000 W and ultrasonic energy having a frequency of 1-1,000 GHz and a power level of 100-5,000 W, or in the absence of a solvent using microwaves having a frequency of 0.1-100 GHz and a power level of 100-4,000 W. There are also provided an apparatus for preparation of metal or non-metal phthalocyanine for carrying out the process described above in the presence or absence of a solvent. COPYRIGHT: (C)2011,JPO&INPIT
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