| 摘要 |
Provided is a method for preparing transition metal oxide nanoparticles from a transition metal as a reactant. The method includes dissolving the transition metal into aqueous hydrogen peroxide to provide peroxi-metallate solution, and then adding a reactive solution containing an alcohol, water and an acid thereto to perform hydrothermal reaction. More particularly, the method for preparing transition metal oxide particles includes: dissolving transition metal powder as a reactant into aqueous hydrogen peroxide to provide a peroxi-metallate solution with a molar concentration of transition metal of 0.001-0.2 M; adding a reactive solution containing an alcohol, water and an acid to the peroxi-metallate solution to provide a mixed solution; and subjecting the mixed solution to hydrothermal reaction to provide transition metal oxide nanoparticles.
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