摘要 |
PROBLEM TO BE SOLVED: To provide a method for producing high-purity bis(3-nitro-4-hydroxyphenyl) represented by formula (1) wherein X represents CH<SB>2</SB>or CHCH<SB>3</SB>, at a high yield, which is an important compound as a raw material for producing a heat resistant polymer or the like. SOLUTION: The high-purity bis(3-nitro-4-hydroxyphenyl) is produced at a high yield by nitrating bis(4-hydroxyphenyl)methane or bis(4-hydroxyphenyl)ethane with nitric acid in an acetonitrile solvent. The compound can easily be made to have high purity by its recrystallization using N-methyl-2-pyrrolidinone. COPYRIGHT: (C)2010,JPO&INPIT
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