发明名称 METHOD FOR PRODUCTION OF CARBON NANOTUBES
摘要 FIELD: nanotechnologies. ^ SUBSTANCE: to synthesise individual carbon nanotubes (CNT), tartrate of the following composition is used: (M1)x(M2)1-xC4H4O64H2O, where Xëñ0.04, M1 represents Fe, Co, Ni or any mixture of them, M2 - alkali-earth metal from the range of Ba, Sr. Tubular reactor is filled with inertial gas and heated up to temperature of tartrate decay, doped tartrate is placed and is decomposed. Produced catalytic system made of powder of alkali-earth metal oxide carrier with particles of metal M1 distributed in it is taken out to cold zone of reactor. Source of carbon is supplied into reactor for synthesis of CNT heated up to 600-1000 C, and produced catalytic system is introduced there as well. On completion of synthesis, supply of carbon source is interrupted, and plant is cooled down to room temperature. ^ EFFECT: invention makes it possible to produce individual carbon nanotubes with narrow distribution of up to 20 nm along diametre. ^ 2 dwg, 5 ex
申请公布号 RU2397951(C1) 申请公布日期 2010.08.27
申请号 RU20090100732 申请日期 2009.01.11
申请人 UCHREZHDENIE ROSSIJSKOJ AKADEMII NAUK INSTITUT NEORGANICHESKOJ KHIMII IM. A.V. NIKOLAEVA SIBIRSKOGOOTDELENIJA RAN 发明人 SHLJAKHOVA ELENA VALENTINOVNA;OKOTRUB ALEKSANDR VLADIMIROVICH;JUDANOV NIKOLAJ FEDOROVICH;BULUSHEVA LJUBOV' GENNAD'EVNA
分类号 B82B3/00;C01B31/02 主分类号 B82B3/00
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