发明名称 METHOD FOR PRODUCING IMIDAZOLIUM SALT
摘要 <P>PROBLEM TO BE SOLVED: To provide a method for producing an imidazolium salt required to have high purity in a high yield. Ž<P>SOLUTION: The production method includes the following steps: (1) a step to quarternize imidazole to obtain an imidazolium salt (A) and produce a reaction solution (C) containing a crude imidazolium salt (B) by an acid exchange reaction; (2) a step to obtain a crude imidazolium salt (B) by removing the solvent from the reaction solution (C); (3) a step to produce an alcohol solution (D) of the crude imidazolium salt (B); and (4) a step to place the alcohol solution (D) under a high pressure of 50-500 MPa in a high-pressure crystallizing apparatus and filter the imidazolium salt crystal (E) while decreasing the pressure at a pressure decreasing rate of 2-100 MPa/min. Ž<P>COPYRIGHT: (C)2010,JPO&INPIT Ž
申请公布号 JP2010037281(A) 申请公布日期 2010.02.18
申请号 JP20080202745 申请日期 2008.08.06
申请人 SANYO CHEM IND LTD 发明人 SAITO KOICHI;SEIKE HIDEO;YAMASHITA TOMOHITO
分类号 C07D233/58 主分类号 C07D233/58
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