发明名称 NMR CryoMAS probe for high-field wide-bore magnets
摘要 All critical circuit components, including the sample coils, are located along with the spinner assembly in a region that may be evacuated to high vacuum for thermal insulation and high-voltage operation. A hermetically sealed spinner assembly simultaneously satisfies the requirements of hermeticity, low total emissivity, rf compatibility, spinning performance, magnetic compatibility, and high filling factor by utilizing metal construction except for the central region near the rf sample coils. Hence, it is possible to maintain high vacuum in the region external to the MAS spinner assembly even over a broad range of bearing and drive gas temperatures. A bundle of optical fibers is provided for tachometry for spin rates up to 60 kHz. The use of alumina disc capacitors allows the noise contributions from the most critical capacitors to be reduced to a minor fraction of the total and simplifies high voltage operation.
申请公布号 US2010026302(A1) 申请公布日期 2010.02.04
申请号 US20070518946 申请日期 2007.11.18
申请人 DOTY SCIENTIFIC, INC. 发明人 DOTY F. DAVID;SHEVGOOR SIDDARTH
分类号 G01R33/44;G01R33/48 主分类号 G01R33/44
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