发明名称 METHOD FOR MANUFACTURING DIALKYLZINC AND DIALKYLALUMINUM MONOHALIDE
摘要 Disclosed is a manufacturing method for dialkyl zinc and dialkyl aluminum monohalide that makes it possible to efficiently manufacture both dialkyl zinc and dialkyl aluminum monohalide of high purity and at a high yield on an industrial scale with a single reaction from zinc chloride and trialkyl aluminum starting materials, while suppressing the production of precipitates in the reaction process and suppressing the adhesion of precipitates to the equipment and the admixture thereof into the product. The manufacturing method for dialkyl zinc and dialkyl aluminum monohalide is a dialkyl zinc and dialkyl aluminum monohalide manufacturing method that causes a reaction between zinc chloride and trialkyl aluminum, and uses trialkyl aluminum with a hydride concentration of 0.01 mass% to 0.10 mass%. Dialkyl zinc that contains essentially no aluminum is separated from the reactants, and then dialkyl aluminum monohalide that contains essentially no zinc is separated.
申请公布号 CA2725412(A1) 申请公布日期 2009.11.05
申请号 CA20092725412 申请日期 2009.04.30
申请人 NIPPON ALUMINUM ALKYLS, LTD. 发明人 TAKAHASHI, HIDEYA;NISHIDA, TADAO;KOGA, SEIJIRO;OKUTANI, MASANORI
分类号 C07F3/06;C07F5/06 主分类号 C07F3/06
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