发明名称 |
METHOD FOR SPINNING AND WASHING ARAMID FIBER AND RECOVERING SULFURIC ACID |
摘要 |
The invention pertains to a method for spinning and washing aramid fiber and for recovering sulfuric acid, using a spinning unit and a sulfuric acid recovery unit, comprising the steps: a) spinning an aramid polymer from a sulfuric acid spin dope to a yarn and coagulating the yarn in a coagulation bath having an inlet for water or diluted sulfuric acid and an outlet for sulfuric acid enriched water; b) washing the yarn with water to obtain washed yarn and washing water containing 0.5-20 wt.% sulfuric acid; c) recycling the sulfuric acid enriched water and optionally the washing water to the sulfuric acid recovery unit; d) increasing the sulfuric acid content of the recycled sulfuric acid enriched water, and optionally the washing water, by evaporation to obtain 20 to 98% sulfuric acid and water; e) mixing the 20 to 98% sulfuric acid with oleum to obtain 98-105% sulfuric acid; f) recycling the 98-105% sulfuric acid to the spinning unit for use as sulfuric acid spin dope. |
申请公布号 |
WO2009053254(A3) |
申请公布日期 |
2009.08.27 |
申请号 |
WO2008EP63576 |
申请日期 |
2008.10.10 |
申请人 |
TEIJIN ARAMID B.V.;KALSBEEK, ESTHER CHRISTINA;BRUINING, WESSEL JOSEPH |
发明人 |
KALSBEEK, ESTHER CHRISTINA;BRUINING, WESSEL JOSEPH |
分类号 |
D01F13/04;D01F6/60 |
主分类号 |
D01F13/04 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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