发明名称 Method for the separation of polymeric by-products from 1,4-butynediol
摘要 The present invention relates to processes for making 1,4-butanediol, 1,4-butenediol, or a mixture thereof by processing 1,4-butynediol in a dynamic mixing apparatus in an inert gas atmosphere at from 25 to 150° C. at a shear rate in the radial gap between rotor and stator of the mixing apparatus of more than 100 000 sec-1; phase separating the processed 1,4-butynediol at a temperature of from 25 to 150° C.; removing a bottom phase to obtain purified 1,4-butynediol; and reacting the purified 1,4-butynediol with hydrogen in the presence of a catalyst.
申请公布号 US7572941(B2) 申请公布日期 2009.08.11
申请号 US20090360278 申请日期 2009.01.27
申请人 BASF AKTIENGESELLSCHAFT 发明人 LORENZ RUDOLF ERICH;PINKOS ROLF;STEINIGER MICHAEL;SCHAEFER GERD
分类号 C07C29/17 主分类号 C07C29/17
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