发明名称 |
Process for obtaining 11-bishomodrim-8(9)-en-12-one |
摘要 |
The invention relates to the field of chemistry, namely to a process for obtaining 11-bishormodrim-8(9)-en-12-one, intermediate compound for obtaining sesqui- and higher terpenoids. The process includes interaction of 11-bishomodrimane-8Alpha -ol-12-one solution in acetonitrile with trimethylsilylmethanesulphonate in equivalent ratio of 1:5, the obtained solution is maintained at the room temperature and continuous agitation up to the termination of the reaction according to the chromatographic control, and then the product is extracted and purified. The product yield is of 80%.
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申请公布号 |
MD3889(B1) |
申请公布日期 |
2009.04.30 |
申请号 |
MD20080000134 |
申请日期 |
2008.05.19 |
申请人 |
INSTITUTUL DE CHIMIE AL ACADEMIEI DE STIINTE A MOLDOVEI |
发明人 |
CUCICOVA CALERIA;ARICU ACULINA;VLAD PAVEL;BARBA ALIC |
分类号 |
C07B35/06;C07C13/48;C07C35/36;C07C49/21 |
主分类号 |
C07B35/06 |
代理机构 |
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主权项 |
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地址 |
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