摘要 |
<p>Preparation of allyl fluoride.. M5-. By fluorination of allyl chloride in the presence of anhydrous dipolar aprotic solvents such as N-methylpyrrolidene, and sulpholanes at high temperature (150-250 degrees C) at atmospheric pressure or under a pressure of 2-20kg/cm2. The preferred temperature range is 160-180 degrees C and the preferred pressure range is 2-5 kg./cm2.</p> |