发明名称 |
METHOD FOR PRODUCING OPTICALLY ACTIVE (4E)-5-CHLORO-2-ISOPROPYL-4-PENTENOIC ACID OR BASIC AMINO ACID SALT THEREOF |
摘要 |
To provide a method for producing an optically active (4E)-5-chloro-2-isopropyl-4-pentenoic acid, a basic amino acid salt thereof or an optically active (4E)-5-chloro-2-isopropyl-4-pentenoic acid ester with high yield and high optical purity by simple operation. An optically active (4E)-5-chloro-2-isopropyl-4-pentenoic acid is obtained by precipitating a basic amino acid salt of optically active (4E)-5-chloro-2-isopropyl-4-pentenoic acid from a solvent solution containing an optical isomer mixture of (4E)-5-chloro-2-isopropyl-4-pentenoic acid and an optically active basic amino acid or a salt thereof, and then the basic amino acid salt of optically active (4E)-5-chloro-2-isopropyl-4-pentenoic acid is subjected to a desalting reaction. Further, an esterification reaction is carried out to obtain an optically active (4E)-5-chloro-2-isopropyl-4-pentenoic acid ester.
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申请公布号 |
US2008255385(A1) |
申请公布日期 |
2008.10.16 |
申请号 |
US20080139553 |
申请日期 |
2008.06.16 |
申请人 |
ASAHI GLASS COMPANY, LIMTED |
发明人 |
MAKINO MAYUMI;SAKATA KAZUHISA;MATSUMURA YASUSHI |
分类号 |
C07C69/65;C07C57/03;C07C209/68 |
主分类号 |
C07C69/65 |
代理机构 |
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