发明名称 METHODS FOR PRODUCING AND PURIFYING 2-HYDROCARBYL-3,3-BIS(4-HYDROXYARYL)PHTHALIMIDINE MONOMERS AND POLYCARBONATES DERIVED THEREFROM
摘要 Disclosed herein is a method comprising reacting a phenolphthalein material and a primary hydrocarbyl amine in the presence of an acid catalyst to form a reaction mixture comprising 2-hydrocarbyl-3,3-bis(4-hydroxyaryl)phthalimidine, wherein the phenolphthalein material comprises greater than or equal to 95 weight percent phenolphthalein, based on the total weight of phenolphthalein material; quenching the reaction mixture and treating the quenched reaction mixture to obtain a first solid. The first solid is then triturated with a trituration solvent and washed to obtain a second solid, wherein the second solid comprises greater than or equal to 97 weight percent 2-hydrocarbyl-3,3-bis(4-hydroxyaryl)phthalimidine, based on the total weight of the second solid. The second solid may be polymerized to form a polycarbonate.
申请公布号 US2008242829(A1) 申请公布日期 2008.10.02
申请号 US20070694405 申请日期 2007.03.30
申请人 GENERAL ELECTRIC COMPANY 发明人 BASALE RAJSHEKHAR;GANESAN BALAKRISHNAN;GANAPATHY BHOLTA VENKATA RAMA NARAYANAN;KISHAN GURRAM;KULKARNI SURENDRA;NADKARNI PRADEEP;SHANMUGAM SURESH;SINGH RAVINDRA VIKRAM
分类号 C08G65/38;C07D209/32 主分类号 C08G65/38
代理机构 代理人
主权项
地址