发明名称 METHOD FOR OBTAINING 2-ETHYL-3,5-DIMETHYLPIRIDIN
摘要 FIELD: chemistry. ^ SUBSTANCE: invention relates to methods for obtaining heterocyclic compounds, namely, to method for obtaining 2-ethyl-3,5-dimethylpiridin. The method consists in interaction of ammonia with propionic aldehide in presence of catalyst crystalhydrate of lanthanide nitrate Ln(NO3)36H2O, where Ln=Pr, Nd and Tb, molar ratio ammonia: aldehide: catalyst being 50:150:1, at room temperature in DMF during 24 hours. The said compounds are widely used for synthesis of medications, as well as in production of dyes, means of chemical protection of plants, as extragents, sorbents and inhibitors of corrosion. ^ EFFECT: obtaining 2-ethyl-3,5-dimethylpiridin with reduction of content of by-products, increase in target product output to 67%, reduction of output production price. ^ 1 tbl, 1 ex
申请公布号 RU2333908(C1) 申请公布日期 2008.09.20
申请号 RU20070114445 申请日期 2007.04.16
申请人 INSTITUT NEFTEKHIMII I KATALIZA RAN 发明人 BULGAKOV RAMIL' GARIFOVICH;KULESHOV SERGEJ PAVLOVICH;MAKHMUTOV AJNUR RASHITOVICH;DZHEMILEV USEIN MEMETOVICH
分类号 C07D213/09 主分类号 C07D213/09
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