发明名称 PROCESS FOR PREPARING FUMED SILICA DISPERSIONS
摘要 <p>Process for preparing an aqueous dispersion of fumed silica having a pH of 9 to 11.5, the silica having a BET surface area of 30 to 400 m&lt;SUP&gt;2&lt;/SUP&gt;/g and being present in the dispersion at 20% &lt; 40% by weight, characterized in that - water is circulated and via a feed means, and with a rotor/stator machine running, fumed silica powder is introduced in an amount such as to result in a preliminary dispersion having a silica content of between 25% and 70% by weight, and, after all of the silica powder has been added, - the feed means is closed and, at a pH of 2 to 4 and a temperature of 10 to 50°C, shearing is carried out with a shear rate of 10 000 to 30 000 s&lt;SUP&gt;-1&lt;/SUP&gt;, - dilution is carried out with water until the desired silica content is exceeded by 0.1% to 10%, and - subsequently, under the same shearing conditions, an aqueous base is added in an amount and concentration such that the amount needed to attain the desired solids content is reached and a pH of 9 to 11.5 results.</p>
申请公布号 WO2008071466(A1) 申请公布日期 2008.06.19
申请号 WO2007EP59306 申请日期 2007.09.05
申请人 EVONIK DEGUSSA GMBH;LORTZ, WOLFGANG;PERLET, GABRIELE;DIENER, UWE 发明人 LORTZ, WOLFGANG;PERLET, GABRIELE;DIENER, UWE
分类号 C01B33/141;C01B33/26 主分类号 C01B33/141
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