发明名称 METHOD FOR PREPARING MESOPOROUS SILICA AND THE MESOPOROUS SILICA THEREFROM
摘要 <p>Provided are a method for preparing mesoporous silica and mesoporous silica obtained therefrom. The method for preparing mesoporous silica according to the present invention comprises the following steps: a) providing a mixture of a surfactant and 0.5-0.9N HCl; b) preparing silica gel by adding water glass (sodium silicate) to the mixture of the previous step at a temperature of 30-50 °C, with stirring until pH value of 5-7 is obtained; c) removing impurities from the resulted silica gel by washing it with distilled water and filtration; d) drying the resulted silica gel with a microwave heating device; and e) firing the dried silica gel at a temperature of 400 °C or more. Since thus prepared mesoporous silica powder has a specific surface area of 700-900m&lt;SUP&gt;2&lt;/SUP&gt;/g, it can be used as a possible substitute for other porous materials such as activated carbon. Further, owing to its stability at a very high temperature condition such as above 1000 °C, it can be effectively used in various high technology industries as heat insulators for a high temperature use, adsorbents for a high temperature use, catalysts or the like. Since the method of the present invention uses inexpensive water glass as a starting material, it is possible to provide mesoporous silica particles in an economical and efficient way.</p>
申请公布号 WO2007129849(A1) 申请公布日期 2007.11.15
申请号 WO2007KR02234 申请日期 2007.05.07
申请人 YU, MI SUN;MASTERS TECHRON CO., LTD. 发明人 YU, MI SUN
分类号 C01B33/187 主分类号 C01B33/187
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