发明名称 METHOD FOR PRODUCTION OF ALKYLHYDROXYALKYL CELLULOSE
摘要 FIELD: organic chemistry. ^ SUBSTANCE: invention relates to method for production of alkylhydroxyalkyl cellulose by interaction of cellulose with alkylation agent and hydroxyalkylation agent in presence of alkali, namely: a) cellulose is alkalified with 0.9-2.9 eq of alkali metal hydroxide/AGU introducing in form of aqueous alkali in presence of suspending agent containing haloalkyl wherein amount of haloalkyl is calculated according to the next formula: from [alkali metal hydroxide total per AGU] to [alkali metal hydroxide total per AGU plus 4.5]; b) alkali cellulose is react with alkylation agent and hydroxyalkylation agent such as one or more alkylene oxide at temperature of 65C or more; c) alkali metal hydroxide is repeatedly added in form of aqueous alkali; and d) alkylhydroxyalkyl cellulose contained in reaction mixture is isolated and optionally purified. ^ EFFECT: mew method for production of alkylhydroxyalkyl cellulose. ^ 7 cl, 36 ex, 8 tbl
申请公布号 RU2309162(C2) 申请公布日期 2007.10.27
申请号 RU20020119196 申请日期 2002.07.19
申请人 VOLLF VAL'SRODE AG 发明人 DANNKHORN VOL'FGANG;KLOR EHRIK-ANDREHAS;KOVOLLIK MARTIN;SHLEZIGER KHARTVIG;PANNEK JORN-BERND
分类号 C08B11/02;C08B11/08;C08B11/193;C08B15/00 主分类号 C08B11/02
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