发明名称 METHOD FOR PRODUCING DIALKYLIMIDAZOLE AND DIALKYL IMIDAZOLE OBTAINED THEREBY
摘要 PROBLEM TO BE SOLVED: To provide a method for producing dialkylimidazole of high purity by effectively removing impurities and provide the dialkylimidazole obtained thereby. SOLUTION: In this production method, ammonia, primary amine, aldehyde and glyoxal are allowed to react with one another and the resultant crude dialkylimidazole is distilled to produce dialkylimidazole. In this case, the crude dialkylimidazole is treated with heat at a temperature higher than 60°C before the distillation. The heat-treated crude dialkylimidazole is separated into the aqueous layer and the oil layer, then the oil layer is distilled to obtain the dialkylimidazole of high purity. COPYRIGHT: (C)2008,JPO&INPIT
申请公布号 JP2007269658(A) 申请公布日期 2007.10.18
申请号 JP20060095706 申请日期 2006.03.30
申请人 NIPPON SYNTHETIC CHEM IND CO LTD:THE 发明人 NAKAJIMA TAKAHIRO;KAGEYAMA HIDEKI
分类号 C07D233/58 主分类号 C07D233/58
代理机构 代理人
主权项
地址