发明名称 Precipitated Silica
摘要 A precipitated silica with the following physiochemical properties: <tables id="TABLE-US-00001" num="1"> <table frame="none" colsep="0" rowsep="0"> <tgroup align="left" colsep="0" rowsep="0" cols="2"> <colspec colname="1" colwidth="126PT" align="left"/> <colspec colname="2" colwidth="91PT" align="left"/> <THEAD> <ROW> <ENTRY/> </ROW> <ROW> <entry namest="1" nameend="2" align="center" rowsep="1"/> </ROW> </THEAD> <TBODY VALIGN="TOP"> <ROW> <ENTRY>BET surface area</ENTRY> <ENTRY>35 m<SUP>2</SUP>/g to 350 m<SUP>2</SUP>/g</ENTRY> </ROW> <ROW> <ENTRY>BET/CTAB surface area ratio</ENTRY> <ENTRY>0.8 to 1.1</ENTRY> </ROW> <ROW> <ENTRY>Pore volume, PV</ENTRY> <ENTRY>1.6 ml/g to 3.4 ml/g</ENTRY> </ROW> <ROW> <ENTRY>Silanol group density (V<SUB>2 </SUB>= NaOH</ENTRY> <ENTRY>3 ml/(1.5 g) to 9.5 ml/(1.5 g)</ENTRY> </ROW> <ROW> <ENTRY>consumption)</ENTRY> </ROW> <ROW> <ENTRY>Average aggregate size</ENTRY> <ENTRY>250 nm to 1500 nm</ENTRY> </ROW> <ROW> <ENTRY>CTAB surface area</ENTRY> <ENTRY>30 m<SUP>2</SUP>/g to 350 m<SUP>2</SUP>/g</ENTRY> </ROW> <ROW> <ENTRY>DBP value</ENTRY> <ENTRY>150 ml/100 g to 300 ml/100 g</ENTRY> </ROW> <ROW> <ENTRY>V<SUB>2</SUB>/V<SUB>1 </SUB>by Hg porosimetry</ENTRY> <ENTRY>0.19 to 0.46</ENTRY> </ROW> <ROW> <ENTRY>DBP/CTAB</ENTRY> <ENTRY>1.2 to 3.5</ENTRY> </ROW> <ROW> <entry namest="1" nameend="2" align="center" rowsep="1"/> </ROW> </TBODY> </TGROUP> </TABLE> </TABLES> is produced by reacting alkali silicate with mineral acids at temperatures of 60° C. to 95° C. while maintaining a pH of 7.5 to 10.5 and continuously stirring, continuing the reaction to a solids concentration in the precipitation suspension of 90 g/l to 120 g/l, adjusting the pH value to a value of less than or equal to 5, filtering out, washing, drying and optionally grinding or granulating the precipitated silica. The precipitated silica is used as a filler in vulcanizable rubber compounds and vulcanizates.
申请公布号 US2007208127(A1) 申请公布日期 2007.09.06
申请号 US20060536505 申请日期 2006.09.28
申请人 发明人 ESCH HEINZ;GORL UDO;KUHLMANN ROBERT;RAUSCH RALF
分类号 C01B33/14;C08L21/00 主分类号 C01B33/14
代理机构 代理人
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