发明名称 |
METHOD FOR PREPARING METAL-FREE PHTHALOCYANINE |
摘要 |
FIELD: chemical technology. ^ SUBSTANCE: invention relates to a method for synthesis of metal-free phthalocyanine having important and broad practical using. Invention describes a method for synthesis of metal-free phthalocyanine by high-temperature condensation of 3-nitro-5-tert.-butylphthalodinitrile in the presence of lead oxide taken in the amount 0.25-0.27 g, ammonium chloride taken in the amount 0.3-0.33 g and ammonium molybdate taken in the amount 0.02-0.025/1 g of 3-nitro-5-tert.-butylphthalodinitrile at temperature 240-260°C. Invention provides preparing metal-free tetra-(3-nitro-5-tert.-butyl)phthalocyanine with the yield 5% by the simple a single-step technology. ^ EFFECT: improved method of synthesis. ^ 2 ex |
申请公布号 |
RU2301239(C1) |
申请公布日期 |
2007.06.20 |
申请号 |
RU20050141391 |
申请日期 |
2005.12.28 |
申请人 |
GOSUDARSTVENNOE OBRAZOVATEL'NOE UCHREZHDENIE VYSSHEGO PROFESSIONAL'NOGO OBRAZOVANIJA "IVANOVSKIJ GOSUDARSTVENNYJ KHIMIKO-TEKHNOLOGICHESKIJ UNIVERSITET" (IGKHTU) |
发明人 |
GLAZUNOV ALEKSEJ VLADIMIROVICH;SEMEJKIN ALEKSANDR STANISLAVOVICH;SYRBU SERGEJ ALEKSANDROVICH;KOJFMAN OSKAR IOSIFOVICH |
分类号 |
C09B47/067;C07D487/22 |
主分类号 |
C09B47/067 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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