发明名称 Processes for the purification of bis(2-hydroxyethyl)terephthalate
摘要 A method is disclosed for efficiently obtaining BHET of high purity from an EG (ethylene glycol) solution containing crude BHET (bis(2-hydroxyethyl)terephthalate), especially a decomposition product solution obtained by decomposing a polyester containing PET (polyethylene terephthalate) as a main component, by use of EG, while minimizing by-production of impurity components such as DEG (diethylene glycol), DEG ester and oligomers. The decomposition product solution is subjected to crystallization and solid-liquid separation under specific temperature conditions. Further, in accordance with the invention, a method of purifying BHET is taught which comprises evaporation steps of evaporating low-boiling-point components from the decomposition product solution under specific conditions so as to obtain a melt solution and a molecular distillation step of distilling the obtained melt solution under specific conditions so as to obtain a specific fraction.
申请公布号 US7211193(B2) 申请公布日期 2007.05.01
申请号 US20030481989 申请日期 2003.12.24
申请人 PET REBIRTH CO., LTD. 发明人 INADA SHUJI;SATO KIKUCHI
分类号 B01D11/00;C07C67/52;C07C67/54;C08J11/04 主分类号 B01D11/00
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