发明名称 Method for producing 2,2,2-trifluoroethanol
摘要 A method for producing 2,2,2-trifluoroethanol in which a gamma-hydroxybutyric acid salt is reacted with 1,1,1-trifluoro-2-chloroethane to generate 2,2,2-trifluoroethanol is provided. This method leads to increased yields of 2,2,2 -trifluoroethanol, facilitates the separation of salt byproducts and allows the recycling of an aprotic polar solvent. The present invention concerns a method for producing 2,2,2-trifluoroethanol in which a gamma-hydroxybutyric acid salt is reacted with 1,1,1-trifluoro-2-chloroethane in an aprotic polar solvent to generate 2,2,2-trifluoroethanol. This method is characterized in that the gamma-hydroxybutyric acid salt used contains no more than 6 wt % of 4,4'-oxybis(butyric acid).
申请公布号 US7208641(B2) 申请公布日期 2007.04.24
申请号 US20040489362 申请日期 2004.03.12
申请人 TOSOH F-TECH, INC. 发明人 NAGASAKI NORITAKA;KAWAMURA TSUYOSHI;NUKUI KAZUNORI;ARAI SHOJI
分类号 C07C31/24;C07C29/124 主分类号 C07C31/24
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