发明名称 PURIFICATION OF 1,3-PROPANEDIOL
摘要 A process is described for purifying a carbonyl-containing 1,3-propanediol composition, the process comprising: (a) forming a solution of said 1,3-propanediol composition in an acidic aqueous medium; (b) adding a sufficient amount of a base to the aqueous medium to form a basic solution having a pH greater than 7; (c) heating the basic solution under conditions effective to distil a major portion of the water therefrom; and (d) heating the remaining basic solution under conditio ns effective to distil a major portion of the PDO therefrom, to provide a 1,3-propanediol composition having a lower carbonyl content than t he starting carbonyl-containing 1,3-propanediol composition. The process of the invention provides a purified 1,3-propanediol which can b e used as a starting material for a low-colour polyester.
申请公布号 CA2207557(C) 申请公布日期 2007.02.13
申请号 CA19952207557 申请日期 1995.12.15
申请人 SHELL CANADA LIMITED 发明人 KELSEY, DONALD ROSS
分类号 C07C31/20;C07C29/80;C07C29/88 主分类号 C07C31/20
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