发明名称 Process for producing high-purity 2,3-pyridinedicarboxylic acid
摘要 A process for producing 2,3-pyridinedicarboxylic acid having a significantly decreased heavy metal content and capable of satisfying the purity level required for medicinal and agricultural chemicals comprising the steps of: adding at least one sulfur-containing substance selected from a hydrosulfide, a sulfide, a polysulfide, and sulfur to an aqueous solution of 2,3-pyridinedicarboxylic acid or its salt; removing the resulting precipitates from the solution; acidifying the solution with a mineral acid to precipitate 2,3-pyridinedicarboxylic acid; and recovering the precipitates. The aqueous solution to be treated may be an aqueous solution of an alkali metal salt of 2,3-pyridinedicarboxylic acid obtained by alkali decomposition of 2,3-pyridinedicarboxylic acid copper (II) salt, which has been formed or precipitated in a process for producing 2,3-pyridinedicarboxylic acid.
申请公布号 US7157583(B2) 申请公布日期 2007.01.02
申请号 US20030631669 申请日期 2003.07.31
申请人 HEBEI SINOCHEM FUHENG CO., LTD. 发明人 SATO TOSHIO
分类号 C07D213/80;C07D213/803 主分类号 C07D213/80
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