发明名称 METHOD FOR RECOVERING UNREACTED ACRYLIC ACID
摘要 PROBLEM TO BE SOLVED: To provide a method for efficiently recovering acrylic acid from an aqueous solution of the acrylic acid discharged from a production process of a high-boiling acrylic ester. SOLUTION: The method for recovering the acrylic acid is composed of the following steps. a step (1) of adjusting the pH of an aqueous liquid prepared by dissolving the unreacted acrylic acid or its salt produced from the production process of the high-boiling acrylic ester using the acrylic acid and a high-boiling alcohol to≤2, a step (2) of bringing acidic water obtained in the step (1) into contact with an organic solvent and extracting the acrylic acid into the organic solvent, a step (3) of distilling an organic phase obtained in the step (2), distilling off the acrylic acid and thereby affording the acrylic acid from which high-boiling impurities are removed and a step (4) of reusing the acrylic acid obtained in the step (3) in the production of the ester. COPYRIGHT: (C)2006,JPO&NCIPI
申请公布号 JP2006213647(A) 申请公布日期 2006.08.17
申请号 JP20050028195 申请日期 2005.02.03
申请人 TOAGOSEI CO LTD 发明人 SUZUKI JITSUWA;KOYAMA MASANOBU;WAKAYAMA TOSHIYUKI;MIHO SUSUMU
分类号 C07C67/48;C07C67/08;C07C69/54 主分类号 C07C67/48
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