发明名称 |
СПОСОБ ПОЛУЧЕНИЯ АЛЬФА-ГИДРОПОЛИФТОРАЛКАНТИОЛОВ |
摘要 |
FIELD: organic chemistry, chemical technology. ^ SUBSTANCE: invention relates to a method for synthesis of alpha-hydropolyfluoroalkanethiols. Method involves heating benzylpolyfluoroalkyl sulfides with 2-3-fold excess of phosphoric anhydride to temperature 150-180°C. Compounds are used as reagents in organic synthesis in synthesis of fluorine-containing sulfonyl chlorides, sulfoacids and other derivatives. Proposed method provides enhancing yield of end compounds and to simplify technology of the process. ^ EFFECT: improved method of synthesis. ^ 2 cl, 4 ex |
申请公布号 |
RU2004135504(A) |
申请公布日期 |
2006.05.20 |
申请号 |
RU20040135504 |
申请日期 |
2004.12.06 |
申请人 |
Военный университет радиационной, химической и биологической защиты (RU) |
发明人 |
Ермолов Александр Фридрихович (RU);Сизов Алексей Юрьевич (RU);Коврегин Алексей Николаевич (RU);Сердюк Роман Николаевич (RU);Цветков Алексей Александрович (RU) |
分类号 |
C07C323/03 |
主分类号 |
C07C323/03 |
代理机构 |
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代理人 |
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地址 |
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