发明名称 |
Verfahren zur Herstellung von Tris(acetylacetonato)iridium(III) |
摘要 |
A process (A) for the production of tris-(acetylacetonato)-iridium(III) involves: (a) reduction of an iridate(IV) solution to an iridate(III) solution, (b) addition of acetylacetone (acac) or acac salt(s), (c) neutralization to pH 6.5-7.5, (d) heating at about +70 degrees C and/or for about 48 hours and (e) separation of the precipitated complex. An Independent claim is also included for a similar process (B) for the production of the same complex starting from a ca. 0.1-M halo-iridate(IV) solution instead of an iridate(IV) solution. |
申请公布号 |
DE19946545(B4) |
申请公布日期 |
2006.05.04 |
申请号 |
DE1999146545 |
申请日期 |
1999.09.28 |
申请人 |
W.C. HERAEUS GMBH |
发明人 |
WALTER, RICHARD;FRANZ, RENATE |
分类号 |
C07C49/92;B01J23/46;B01J31/22;B01J31/28;C07C45/50;C07C45/77 |
主分类号 |
C07C49/92 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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