发明名称 Neutralization of isophorone nitrile synthesis products
摘要 The present invention relates to a process for preparing 3-cyano-3,5,5-trimethylcyclohexanone (isophoronenitrile) by reacting isophorone with hydrogen cyanide in the presence of a base as a catalyst to obtain a crude isophoronenitrile product, and subsequently distilling the crude isophoronenitrile product, with the addition before distillation of at least one specific sulfonic acid or specific carboxylic acid. In addition, the present invention relates to the use of a specific sulfonic acid or of a specific carboxylic acid as a neutralizing agent before distillation of a crude isophoronenitrile product which has been obtained by reacting isophorone with hydrogen cyanide in the presence of a base as a catalyst, in order to avoid precipitates in the neutralization of the base used as a catalyst with an acid.
申请公布号 US2006058544(A1) 申请公布日期 2006.03.16
申请号 US20050539134 申请日期 2005.06.16
申请人 BASF AKTIENGESELLSCHAFT 发明人 OFTRING ALFRED;BRAUN GEROLD
分类号 C07C253/08;C07C253/10;C07C255/46 主分类号 C07C253/08
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