发明名称 |
METHOD FOR PREPARING 3beta-ACETOXY-20,20-DIMETHOXYNORTARAXASTANE |
摘要 |
FIELD: organic chemistry, chemical technology. ^ SUBSTANCE: invention relates to novel method for synthesis of 3beta-acetoxy-20,20-dimethoxynortaraxastane of the formula (1): . Method is carried out by interaction of 3beta-acetoxy-20-methylenetaraxastane in chloroform solution with ozone excess in the mole ratio 3beta-acetoxy-20-methylenetaraxastane : ozone = 1:1.5 with addition of methanol, at room temperature and stirring. The yield of the end product is 68%. ^ EFFECT: improved method of synthesis. ^ 2 cl, 1 ex |
申请公布号 |
RU2316562(C1) |
申请公布日期 |
2008.02.10 |
申请号 |
RU20060113901 |
申请日期 |
2006.04.24 |
申请人 |
INSTITUT NEFTEKHIMII I KATALIZA RAN |
发明人 |
AKHMETOVA VNIRA RAKHIMOVNA;SHAKUROVA EHL'VIRA RIFOVNA;KHALILOVA ALIJA ZUFAROVNA;KHALILOV LEONARD MUKHIBOVICH |
分类号 |
C07J53/00;C07J63/00 |
主分类号 |
C07J53/00 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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