发明名称 |
A METHOD FOR THE PREPARATION OF PHENYL-M-TOLYLPHOSPHATE SALT OF DI(2-CHLOROETHYL) AMINE |
摘要 |
A method for the preparation of phenyl-m-tolylphosphate salt of di(2-chloroethyl) amine comprises the reaction of phenyl-m-tolylphosphoric acid with di(2- chloroethyl) amine. A synthesis is performed in one stage without isolation of intermediate substances in the interaction of hydrochloric salt ofdi(2- chloroethyl) amine, chloroanhydride phenyl-m- tolylphosphoric acid and triethylamine in the aqueous medium. The crystalline product is isolated of reaction mixture by filtration and cleaning.
|
申请公布号 |
UA12338(U) |
申请公布日期 |
2006.02.15 |
申请号 |
UA20050001156 |
申请日期 |
2005.02.09 |
申请人 |
SCIENTIFIC-AND-PRACTICAL CENTER OF ENDOVASCULAR NEURORADIOSURGERY OF AMSU |
发明人 |
SCHEHLOV VIKTOR IVANOVYCH;KUZMENKO IVAN YOSYPOVYCH;SCHEHLOV DMYTRO VIKTOROVYCH |
分类号 |
A61K31/131;A61K31/661;A61P35/00;C07C211/03;C07F9/12;(IPC1-7):A61K/131;A61K/661;A61P/00;C07C/03;C07F/12 |
主分类号 |
A61K31/131 |
代理机构 |
|
代理人 |
|
主权项 |
|
地址 |
|