发明名称 METHOD FOR PREPARING TRIS-(2-HYDROXYETHYL)-AMMONIUM-ORTHO-CRESOXYACETATE
摘要 FIELD: organic chemistry, chemical technology. ^ SUBSTANCE: invention relates to preparing biologically active compounds used in agriculture and animal husbandry. Tris-(2-hydroxyethyl)-ammonium-o-cresoxyacetate is prepared by interaction of triethanolamine with o-cresozyacetic acid in the solvent medium under conditions of three-stage temperature effect. At the first stage the process is carried out at the solvent boiling point, at the second stage at temperatures 81-85°C, and at the three stage at temperatures 73-77°C. The process is carried out in the vertical device fitted with three heating zones and rotor with control number of revolution and consisting of shaft with movable vanes. Invention provides simplified method due to diminishing number of the process stages. ^ EFFECT: improved preparing method. ^ 2 cl, 3 ex
申请公布号 RU2268879(C1) 申请公布日期 2006.01.27
申请号 RU20040114583 申请日期 2004.05.12
申请人 发明人 ERMAKOV ANATOLIJ ALEKSANDROVICH;ERMAKOV SERGEJ ANATOL'EVICH;POLOMARCHUK NINA IVANOVNA
分类号 C07C215/40 主分类号 C07C215/40
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