| 摘要 |
A hydrometallurgical process based on pressure leaching at elevated temperature for recovering nickel from nickel oxide ores, characterized by a simplified and efficient process as a whole, realizing a simplified leaching stage, reduced neutralizer consumption and precipitate production in the neutralization stage, and efficient use of recycled water. The hydrometallurgical process of the present invention, comprising a leaching stage which stirs the slurried ore in the presence of sulfuric acid at 220 to 280° C. to produce the leached slurry; solid-liquid separation stage which washes the leached slurry in multi-stages to produce the pregnant liquor and leached residue, the former containing nickel and cobalt; neutralization stage which treats the pregnant liquor in the presence of calcium carbonate incorporated to keep the pH level at 4 or less, while suppressing oxidation of the liquor, to produce the neutralization precipitate slurry and mother liquor for nickel recovery, the former containing trivalent iron; and a sulfide precipitation stage which blows hydrogen sulfide gas into the mother liquor to produce the sulfide solution and barren liquor, the former containing nickel and cobalt.
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