发明名称 Production of bisphenol-A with reduced sulfur content
摘要 A process for the production of bisphenol-A having low concentration of sulphur is disclosed. The process comprise a) reacting phenol with acetone in the presence of a sulfonic acid ion exchanger to form a product mixture containing water, bisphenol-A/phenol adduct, phenol and sulfurous particles, and b) filtering the product mixture to separate the sulfurous particles to obtain a purified product mixture that contains water, phenol and bisphenol-A/phenol adduct. In one embodiment of the process further comprise distilling the purified product mixture to remove the water to obtain a first material system that contains said adduct and phenol, crystallizing the adduct, and removing the phenol by filtration using a filtering apparatus to obtain crystalline adduct. In a yet additional embodiment the process comprise crystallizing the purified product mixture to obtain a second material system that contains crystalline adduct, water and phenol and removing the phenol and water by filtration using a filtering apparatus to obtain crystalline adduct.
申请公布号 US2005215833(A1) 申请公布日期 2005.09.29
申请号 US20050043800 申请日期 2005.01.26
申请人 NEUMANN RAINER;BLASCHKE ULRICH;WESTERNACHER STEFAN 发明人 NEUMANN RAINER;BLASCHKE ULRICH;WESTERNACHER STEFAN
分类号 C07C37/20;C07C37/82;C07C37/84;C07C39/16;C08G64/06;(IPC1-7):C07C39/16 主分类号 C07C37/20
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