发明名称 Method for producing 2,6-dimethylnaphthalene
摘要 An object of the present invention is to provide a method for manufacturing 2,6-DMN, in which even when a mixture containing DMN isomers which includes 5 wt % or more of 2,7-DMN is used, a highly pure 2,6-DMN can be obtained. The method for manufacturing the highly pure 2,6-dimethylnaphthalene of the present invention comprises performing cooling crystallization of a mixture containing dimethylnaphthalenes which includes 2,6-dimethylnaphthalene, performing solid-liquid separation to obtain a solid component, and washing the solid component using a solvent, wherein the solid-liquid separation performed after the cooling crystallization includes press filtration. In the present invention, the pressure of the press filtration is preferably 10 kg/cm<SUP>2 </SUP>or more, and according to the method of the present invention, even when a DMN mixture containing 5 wt % or more of 2,7-DMN is used as a feedstock, a highly pure 2,6-DMN can be manufactured, and in addition, even when a DMN mixture containing less than 25 wt % of 2,6-DMN is processed by cooling crystallization, a highly pure 2,6-DMN can be manufactured.
申请公布号 US6894202(B1) 申请公布日期 2005.05.17
申请号 US20020069502 申请日期 2002.02.27
申请人 KOBE STEEL, LTD. 发明人 YAMAMOTO KOJI;YAMAMOTO SEIICHI;TANAKA TAKEHARU;MOTOYUKI MASAHIRO;YOSHIDA SHINGO
分类号 C07C7/14;C07C15/24;(IPC1-7):C07C7/14 主分类号 C07C7/14
代理机构 代理人
主权项
地址