发明名称 |
Extraction process for removal of impurities from mother liquor in the synthesis of carboxylic acid |
摘要 |
A method for removing impurities from a mother liquor comprising a carboxylic acid, a metal catalyst, impurities by (a) evaporating the mother liquor comprising a carboxylic acid, a metal catalyst, impurities and a solvent in a first evaporator zone to produce a vapor stream and a concentrated mother liquor stream;(b) evaporating the concentrated mother liquor stream in a second evaporator zone to form a solvent rich stream and a super concentrated mother liquor stream; (c) mixing in a mixing zone a water-solvent solution and optionally an extraction solvent with the super concentrated mother liquor stream to form an aqueous mixture;(d) optionally separating organic impurities from the aqueous mixture in a solid-liquid separation zone to form a purified aqueous mixture; and (e) extracting the aqueous mixture or purified aqueous mixture with an extraction solvent in an extraction zone to form an extract stream and the raffinate stream. |
申请公布号 |
EP1484306(A1) |
申请公布日期 |
2004.12.08 |
申请号 |
EP20040011594 |
申请日期 |
2004.05.14 |
申请人 |
EASTMAN CHEMICAL COMPANY |
发明人 |
LIN, ROBERT;DE VREEDE, MARCEL |
分类号 |
B01D11/04;B01J23/94;B01J38/00;B01J38/04;B01J38/06;C07B61/00;C07C51/265;C07C51/42;C07C51/48;C07C63/26 |
主分类号 |
B01D11/04 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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