发明名称 METHOD FOR PURIFYING AND PRODUCING 2,5-BIS(ISOCYNATOMETHYL)-1,4-DITHIANE
摘要 PROBLEM TO BE SOLVED: To provide a method for purifying a mixture containing BIMD [2,5-bis(isocyanatomethyl)-1,4-dithiane] with which the high-purity BIMD with slight discoloration can be obtained and to provide a method for industrially advantageously producing the BIMD. SOLUTION: The method for purifying the BIMD is to isolate the BIMD by distilling the mixture containing the BIMD. The method for purifying the BIMD comprises a step of treating the mixture containing the BIMD with a removing material for colored substances. The method comprises a step of carrying out a phosgenation reaction of an inorganic acid salt of BAMD [2,5-bis(aminomethyl)-1,4-dithiane], a step of treating the resultant phosgenation reaction product with the removing material for the colored substances and a step of distilling the reaction product treated with the removing material for the colored substances and isolating the BIMD. Thereby, the high-purity BIMD with the slight discoloration can be isolated/purified by simple operation without adding a great change to a conventional method for production. COPYRIGHT: (C)2004,JPO&NCIPI
申请公布号 JP2004256398(A) 申请公布日期 2004.09.16
申请号 JP20030046046 申请日期 2003.02.24
申请人 NIPPON SODA CO LTD 发明人 SUGIMOTO YOSHIAKI;MIYAKI MAKOTO;KOBAYASHI MAKOTO
分类号 C07D339/08;(IPC1-7):C07D339/08 主分类号 C07D339/08
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