发明名称 |
METHOD FOR THE SYNTHESIS OF METHYL-TRI-OXO-RHENIUM |
摘要 |
<p>A method for the synthesis of methyltrioxorhenium is described, wherein 0.5-1.5 moles of dirhenium heptaoxide are reacted with 1-3 moles of tetramethyl tin in the presence of 1-3 moles of chlorotrimethyl silane. The synthesis is carried out in the dark for approximately 24 hours in a polar aprotic organic solvent, preferably in acetonitrile.</p> |
申请公布号 |
WO2004076469(A1) |
申请公布日期 |
2004.09.10 |
申请号 |
WO2004IT00060 |
申请日期 |
2004.02.16 |
申请人 |
CHEMI SPA;TURCHETTA STEFANO;MASSARDO PIETRO;TUOZZI ANGELA |
发明人 |
TURCHETTA STEFANO;MASSARDO PIETRO;TUOZZI ANGELA |
分类号 |
C07F13/00;(IPC1-7):C07F13/00 |
主分类号 |
C07F13/00 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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