发明名称 Process for producing magnetite particles
摘要 This invention relates to a process for producing magnetite particles having a coercivity of 6.366 kA/m to 10.345 kA/m (=80 to 130 Oe) and an octahedral particle shape, comprising heating an alkaline component and an iron(II) component in the form of an aqueous solution to a temperature of 50° C. to 100° C., whereby the molar ratio of iron(II) component to one equivalent of alkaline component is 0.38 to 0.45, and treating the suspension with an oxidizing agent at a rate of oxidation of 20 to 50 mol. % Fe(II)/h until the iron compound has an Fe(III) content of more than 65 mol. %, and then again adding an Fe(II) component in the form of an aqueous solution at a molar ratio of Fe(II) to one equivalent of total alkaline component used is 0.47 to 0.49, and treating the suspension with an oxidizing agent, at a rate of oxidation is 20 to 50 mol. % Fe(II)/h until the iron compound has an Fe(III) content of more than 65 mol. %, and filtering the suspension, and washing, drying and grounding the residue.
申请公布号 US6767529(B2) 申请公布日期 2004.07.27
申请号 US20020047315 申请日期 2002.01.14
申请人 BAYER AKTIENGESELLSCHAFT 发明人 MEISEN ULRICH
分类号 G03G9/083;C01G49/08;C09C1/24;H01F1/20;H01F1/36;(IPC1-7):C01G49/00 主分类号 G03G9/083
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