发明名称 Purifying 2,3-pyridine-dicarboxylic acid used as intermediate for e.g. drugs, by treatment in solution with sulfur source, removal of precipitate and precipitation with acid, giving low heavy metal content
摘要 Production of 2,3-pyridine-dicarboxylic acid (I) having a reduced heavy metal content comprises: (a) adding at least one sulfur source comprising hydrosulfides, sulfides, polysulfides or sulfur, to a solution of (I) or its salts; (b) removing the obtained precipitate from the solution; (c) acidifying the solution with mineral acid, and (d) recovering the precipitated (I).
申请公布号 DE10341864(A1) 申请公布日期 2004.06.03
申请号 DE20031041864 申请日期 2003.09.09
申请人 SUMIKIN AIR WATER CHEMICAL INC., TOKYO;HEBEI SINOCHEM FUHENG CO., LTD. 发明人 SATO, TOSHIO
分类号 C07D213/80;C07D213/803;(IPC1-7):C07D213/79 主分类号 C07D213/80
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